Authenticity green coffee bean species and geographical origin using near-infrared spectroscopy combined with chemometrics

To prevent the adulteration of agricultural resources and provide a solution to enhance the green coffee bean supply chain, authentication using the near-infrared spectroscopy (NIRS) technique was investigated. Partial least square with discrimination analysis (PLS-DA) models combined with various preprocessing methods were built from NIR spectra of 153 Vietnamese green coffee samples. The model combined with the standard normal variate and the first order of derivative yielded excellent performance in predicting coffee species with the error cross-validation of 0.0261. PLS-DA model of mean centre and first-order derivative spectra also yielded good performance in verifying geographical indication of green coffee with the error of 0.0656. By contrast, the predicting abilities of post-harvest methods were poor. The overall results showed a high potential of the NIRS in online authentication practices.     

亲水作用色谱-串联质谱法测定动物源运动食品中3种氨基糖苷类抗生素的残留量

该研究建立了一种亲水交互作用色谱-串联质谱（HILIC-MS/MS）法测定动物源运动食品中潮霉素B、新霉素、安普霉素3种氨基糖苷类抗生素残留量的方法。结果表明，样品经Sielc Obelisc R柱分离，采用0.1%甲酸水溶液-乙腈梯度洗脱，可以实现3种目标物组分的分离。在此条件下，3种氨基糖苷类抗生素在5～500 ng/mL的质量浓度范围内线性关系良好，相关系数R2为0.999 5～0.999 9，检出限均为15 μg/kg，定量限均为50 μg/kg，保留时间的日间和日内相对标准偏差（RSD）分别为3.5%～7.9%和3.5%～4.1%，峰面积的日间和日内RSD分别为3.6%～7.4%和3.2%～3.9%，加标回收率为85.7%～93.6%，回收率试验结果的RSD为3.1%～5.2%。该方法可以满足动物源运动食品中3种氨基糖苷类抗生素的检测需求。     

北部湾盆地福山凹陷CO2气成因探讨

北部湾盆地福山凹陷油气钻探中发现了高含CO₂气的天然气气藏。对CO₂气稳定碳同位素、伴生稀有气体氦和氩同位素进行了分析研究，结果显示，福山凹陷CO₂气稳定碳同位素偏重，(13C_CO2为-5.01～-10.08‰，绝大多数样品大于-7.0‰，为无机成因CO₂气特征；伴生稀有气体氦同位素³He/⁴He值为(4.74~5.03)×10^-6，R/Ra值为3.38～3.59；伴生稀有气体氩同位素⁴⁰Ar/³⁶Ar值为1881～2190，也显示出幔源或壳幔混合CO₂气的特征。综合判定认为，福山凹陷CO₂为壳幔混合成因。始新统流沙港组岩浆岩体分布特征与CO₂气藏分布范围基本一致，也表明幔源-岩浆可能是福山凹陷CO₂气的主要来源。与南海北部边缘盆地其它地区如珠江口盆地西部、琼东南盆地东部CO₂气成因一致，都为幔源-岩浆来源，或壳幔混合来源。     

HLA仿真系统因果追溯性设计

随着仿真系统变得日益复杂，基于仿真数据人为的进行因果追溯已经变得越来越凼难，所以必须对原有的仿真系统进行因果追溯性设计，使自动或半自动追溯凶果成为可能。为此，首先确定了因果关系追溯的整体思路，然后面对普遍使用的高层体系结构HLA分印仿直系统，深入分析对象类和交互类两类交互数据以及交互特点，井详细划分行为事件及因果关系类型；对HLA仿真系统中关键的联邦对象模型FOM以及仿真器进行扩展设计，从而实现系统的因果追溯性，为仿真因果追溯分析提供必要的数据。最后提出保证因果追溯需要注意的几项设计原则，并对设计所能够支持的应用做出展望。     

关于后张预应力混凝土结构优化设计的几个问题

结合UP软件编程实践，本文对后张预应力混凝土结构计算程序中引入优化功能的意义进行了论述，提出了预应力筋与普通钢筋之间的最优搭配关系，优化原点概念及相关影响因素，列出了优化计算程序所应涉及的基本计算内容，并对当前后张预应力混凝土结构设计中的一些观点提出了不同意见。     

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本文应用天然气中甲烷、乙烷的碳同位素,甲烷的氢同位素,汞含量及天然气成分等指标,探讨了四川盆地天然气成因分类;并结合地质情况对气源层进行了探讨。     

秦牧散文的文体改造与源流

秦牧作为17年时期重要的散文家之一，其成绩是与他所自觉进行的文体改造分不开的。秦牧的身份和处境使得他的文体改造颇为顺利。秦牧17年文体改造体现在特写强调、抒情风味、辨证色彩三个方面，这与当时的文风密切相关。秦牧的文体改造延续了学者散文的文脉，也印证了文体改造在文学史上的积极意义。     

柴达木盆地断裂上下盘油气差异聚集效应与成因

断裂沟通含油气盆地不同层位、不同时代的烃源岩和生储盖组合，成为连接烃源岩和各种圈阔的重要渠道，导致了多种类型的与断裂有关的油气藏的形成。柴达木盆地的断裂控烃特征明显，断裂上下盘油气差异聚集现象十分普遍，不同构造系统区具有不同的油气差异聚集机理和模式。其根本原因是断裂上下盘具有不同的地质特征和油气运聚成藏条件，它们往往是互为消长的关系。油气是富集在断裂的上盘，还是聚集在断裂的下盘，取决于具体的地质条件。     

Mutual recognition of the results of measurements and tests and formation of a world-wide metrology system

The main prerequisites are considered in a historical aspect and steps ate taken in creating a world-wide metrology system with the aim of providing conditions for the mutual recognition of measurement results. __________ Translated from Izmeritel’naya Tekhnika, No. 11. pp. 59–62, November, 2007.     

Prolonged poststrike elevation in tongue-flicking rate with rapid onset in gila monster,Heloderma suspectum: Relation to diet and foraging and implications for evolution of chemosensory searching

Experimental tests showed that poststrike elevation in tongue-flicking rate (PETF) and strike-induced chemosensory searching (SICS) in the gila monster last longer than reported for any other lizard. Based on analysis of numbers of tongue-flicks emitted in 5-min intervals, significant PETF was detected in all intervals up to and including minutes 41–45. Using 10-min intervals, PETF lasted though minutes 46–55. Two of eight individuals continued tongue-flicking throughout the 60 min after biting prey, whereas all individuals ceased tongue-flicking in a control condition after minute 35. The apparent presence of PETF lasting at least an hour in some individuals suggests that there may be important individual differences in duration of PETF. PETF and/or SICS are present in all families of autarchoglossan lizards studied except Cordylidae, the only family lacking linguallly mediated prey chemical discrimination. However, its duration is known to be greater than 2-min only in Helodermatidae and Varanidae, the living representatives of Varanoidea. That prolonged PETF and SICS are typical of snakes provides another character supporting a possible a varanoid ancestry for Serpentes. Analysis of 1-min intervals showed that PETF occurred in the first minute. A review of the literature suggests that a pause in tongue-flicking and delay of searching movements are absent in lizards and the few nonvenomous colubrid snakes tested. The delayed onset of SICS may be a specific adaptation of some viperid snakes to allow potentially dangerous prey to be rendered harmless by venom following voluntary release after envenomation and preceding further physical contact with the prey.